monolithic silica

Monolithic silica columns for high-efficiency chromatographic ...

2002年8月2日  This type of monolithic silica columns, Chromolith, is commercially available at 5- or 10-cm length. The silica network structure must be attached to the tube wall to

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Recent Progress in Monolithic Silica Columns for High-Speed

2022年12月11日  Monolithic silica columns possess a network of structures consisting of porous silica skeletons with a bimodal pore arrangement, in which large through-pores

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Advances in monolithic silica columns for high-performance

2017年9月3日  This review attempts to give an overview of three different types of monolithic columns, i.e. silica-based, polymer-based, and hybrid monolithic column.

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In situ one-step construction of monolithic silica aerogel

2020年8月15日  Monolithic silica aerogel-based composite PCMs possess excellent shape stability and high compressive strength (11 MPa). • The silica aerogel-based composite

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One-pot synthesis of monolithic silica-cellulose aerogel applying

2021年7月26日  The monolithic silica-cellulose aerogel can be synthesized from low modulus (1.5) silicate sol-gel process. The embedded CO 2 emission of this new aerogel

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Inverse Analysis of Monolithic Silica Aerogel’s

2023年10月31日  In this paper, the monolithic silica aerogel’s temperature of hot surface is measured with limited probes, and then the thermal conductivity is obtained by Fourier’s

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Versatile Double-Templating Synthesis Route to Silica

2003年5月13日  Monolithic silica exhibiting a trimodal, hierarchical pore structure has successfully been prepared via sol−gel-processing. Monolithic bodies with

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Recent advances in sol–gel synthesis of monolithic

2018年4月18日  More recently, the preparation of clear monolithic RE–P codoped silica glasses from solutions containing fumed silica has been reported . The cosolvent-free synthesis of macroporous silica gels from

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One-step eco-friendly fabrication of classically monolithic silica ...

2018年9月25日  This was the first report that the classically monolithic silica aerogel with both nanoscale coherent skeletons and pores was achieved via eco-friendly water

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Longevity and other practical benefits of monolithic silica

2023年8月15日  This part is devoted to the applications of the monolithic silica columns in medium-pressure flow systems, where the column's low back pressure enables hyphenate separation with other automated analytical steps in a single manifold. During the SIC evolution, various monolithic columns of 25–100 mm lengths, including very short guard

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HPLC Column Monolith Phenomenex Onyx

Octadecyl silane ligands are bound to the monolithic silica surface, making for a general hydrophobic phase for viscous and dirty samples. 3 Phases Reversed Phase 3 Monolithic C18 Monolithic C8 Monolithic HD-C18 技术文档 技术规格 FAQ 固定相 ...

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Recent Progress in Monolithic Silica Columns for High-Speed

2022年12月11日  Monolithic silica columns have greater (through-pore size)/(skeleton size) ratios than particulate columns and fixed support structures in a column for chemical modification, resulting in high-efficiency columns and stationary phases. This review looks at how the size range of monolithic silica columns has been expanded, how high-efficiency

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Monolithic silica columns for high-efficiency chromatographic ...

2002年8月2日  Monolithic silica columns prepared from tetraalkoxysilane by a sol–gel method showed high efficiency and high permeability on the basis of the small-sized silica skeletons, large-sized through-pores, and resulting through-pore size/skeleton size ratios much larger than those found in a particle-packed column.

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One-pot synthesis of monolithic silica-cellulose aerogel applying

2021年7月26日  The monolithic silica-cellulose aerogel can be synthesized from low modulus (1.5) silicate sol-gel process. The embedded CO 2 emission of this new aerogel is significantly reduced, reflected by the obviously lower footprint of olivine sodium silicate compared to commercial water glass, namely 2.481 tCO 2 /t and 5.517 tCO 2 /t,

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Methyltrimethoxysilane based monolithic silica aerogels via ambient ...

2007年3月23日  In summary, monolithic silica aerogels can easily be prepared by the sol–gel polymerization of methyltrimethoxysilane precursor followed by the drying of the gels at the ambient pressure. The in situ attachment of methyl groups to the siloxane backbone and the low degree of silica polymerization make the silica network easily deformable that ...

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Recent advances in sol–gel synthesis of monolithic silica and silica ...

2018年4月18日  Synthesis of monolithic silica gels and glasses is a basic research topic in the area of sol–gel processing. Although fracture during the drying of wet gels is still a major problem, it has largely been solved by supercritical drying and the addition of particulate silica fillers. On the other hand, the reduction of the surface tension of the ...

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Preparation of Monolithic Silica Aerogel for Fenestration

The ability of a rapid supercritical extraction (RSCE) process implemented in an industrial hot press to produce silica aerogel monoliths (AMs) with properties suitable for use in fenestration products was investigated. The effects of hot-press processing parameters such as press force and heat-up and cool-down rates on the size (area) and quality (presence

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A new route to aerogels: Monolithic silica cryogels

2012年2月1日  Highlights We have explored several routes to synthesize monolithic silica cryogels. We highlight two routes to monoliths with similarities to the corresponding aerogels. Low freezing temperatures and fast cooling rates favor monolithicity. Uniform networks and a high degree of 3-D cross-linking correlate with monolithicity. Compared

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Mechanical properties of monolithic silica aerogels made

2014年1月1日  We report the preparation and characterization of a broad range of hydrophobic monolithic silica aerogels and xerogels made from polyethoxydisiloxane (PEDS-P 750E20) precursors.Transparent silica aerogels with densities spanning ≈ 0.05 to >0.32 g/cm 3 were synthesized and the effects of density on the mechanical,

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Monolithic Silica SnG Inc.

Monolithic silica has excellent thermal stability, mechanical strength and chemical stability because of its unique mesh-like skeleton. Monolithic silica is pure silica gel and withstands high temperatures exceeding 800 ℃.

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Inverse Analysis of Monolithic Silica Aerogel’s

2023年10月31日  Thermal conductivity is the only measurable parameter for a simple and restricted steady-state apparatus. To deeply explore monolithic silica aerogel’s thermophysical properties, not limited to thermal conductivity, we developed a novel differentiable learning (DL) method to evaluate unsteady-state thermal insulation

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In situ one-step construction of monolithic silica aerogel

2020年8月15日  This monolithic silica aerogel-based composite PCMs could prolong heat preservation duration due to the synergistic effect between low thermal conductivity and high latent heat of composite PCMs, showing potential promise for direct application to the thermal insulation and thermal protection device. More importantly, this in situ one-step ...

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Antibody-coupled monolithic silica microtips for highthroughput ...

2014年8月29日  Here we constructed anti-CD9 antibody-coupled highly porous monolithic silica microtips which allowed automated rapid and reproducible exosome extraction from multiple clinical samples. We applied ...

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Nanoparticle Formulation Composition Analysis by Liquid

2022年12月22日  Our study identifies the viability of reversed-phase monolithic silica in the chromatography of both small drug molecules and particularly pharmapolymers in a repeatable and simultaneous fashion, and can provide a valuable strategy for analysis of diverse precursor polymer systems and drug components in multifunctional drug

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Development of hydrophobic and optically transparent monolithic silica ...

2016年10月26日  In the present paper, highly transparent, monolithic and hydrophobic silica aerogel monoliths were prepared by using tetraethoxysilane (TEOS) as precursor and methyltriethoxysilane (MTES) as co-precursor with different MTES/TEOS molar ratios (M) by two-step acid–base catalyzed sol–gel process followed by supercritical alcohol drying.

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Thermoresponsive Polymer Brush on Monolithic-Silica-Rod

2019年12月12日  The prepared monolithic silica-rod columns were also characterized by chromatographic analysis. PIPAAm-brush-modified monolithic silica-rod columns were able to separate hydrophobic steroids with a short analysis time (10 min), compared to PIPAAm-brush-modified silica-beads-packed columns, because of the horizontally limited diffusion

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Optical and visual experimental characterization of a glazing

2019年5月1日  Monolithic silica aerogel is an innovative transparent material with attractive optical, thermal, and acoustic insulating properties. Granular silica aerogel is already available on the market in some commercial glazings. The fabrication process for aerogel monoliths has not been developed at the industrial scale, due to the high cost and to ...

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Monolithic silica columns with chemically bonded tert ...

2004年5月21日  An enantioselective silica rod type chiral stationary phase (CSP) is presented as a novel combination of the well-known enantiomer separation properties of immobilized tert-butyl-carbamoylquinine chiral anion-exchanger selector with the unique properties of monolithic silica material.The chromatographic behavior of the tert-butyl

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Mechanical properties of monolithic silica aerogels made

DOI: 10.1016/J.MICROMESO.2013.08.029 Corpus ID: 97958498; Mechanical properties of monolithic silica aerogels made from polyethoxydisiloxanes @article{Wong2014MechanicalPO, title={Mechanical properties of monolithic silica aerogels made from polyethoxydisiloxanes}, author={Joanna C.H. Wong and Hicret Kaymak and

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